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Synthesis and crystal structure of a novel multimodal ligand, 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine, and its copper(I) complex, {[Cu3L2](PF6)3° 3H2O} (1)
dipyridyl ketone metal complexes N-donor ligands
2010/12/3
The single crystal X-ray structure of the novel multimodal ligand 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine, C34H28N10 (L), was determined at 120 (2) K. The ligand pos...
Synthesis and crystal structure of a novel multimodal ligand, 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine and its copper(I) complex, {[Cu3L2](PF6)3?3H2O} (1)
Bipyridine derivatives hydrazone dipyridyl ketone metal complexes
2010/10/19
The single crystal X-ray structure of the novel multimodal ligand 6,6’-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2’-bipyridine, C34H28N10 (L), was determined at 120 (2) K. The ligand pos...
Synthesis, Spectroscopic Characterization, Mass Spectrometry and Crystal Structure of N-{[(4-bromophenyl) amino]carbonothioyl}benzamide
Thiourea derivative X-ray structure determination mass fragmentation
2010/10/19
N-{[(4-bromophenyl)amino]carbonothioyl}benzamide was synthesized and characterized by IR, 1 H- and 13C-NMR, mass spectrometry, and elemental analysis. The crystal structure was determined from single ...
The Effect of Electrocatalytic Activity and Crystal Structure of PbO2 Surfaces on Polyphenylene Oxide (PPO) Production in Acetonitrile
a-PbO2 b -PbO2 phenol electrocatalysis PPO
2010/4/9
The crystallographic nature of PbO2 films was changed by optimizing the electrolysis conditions in an electrodeposition solution of PbO2. These PbO2 films were then used to prepare PPO films. It was d...
The Effect of Electrocatalytic Activity and Crystal Structure of PbO2 Surfaces on Polyphenylene Oxide (PPO) Production in Acetonitrile
a-PbO2 b -PbO2 phenol electrocatalysis PPO
2010/4/9
The crystallographic nature of PbO2 films was changed by optimizing the electrolysis conditions in an electrodeposition solution of PbO2. These PbO2 films were then used to prepare PPO films. It was d...
The Crystal Structure of 2-Nitro-N-(4-nitrophenyl)benzamide
X-ray structure 2-nitro-N-(4-nitrophenyl)benzamide
2010/4/16
2-Nitro-N-(4-nitrophenyl)benzamide was synthesized and characterized by spectroscopy and elemental analysis. The crystal structure was determined from single-crystal X-ray diffraction data. It crystal...
Dinuclear Molybdenum Tetracarbonyl Complexes of Tetradentate Nitrogen Ligands and Intermolecular Hydrogen Bonding in the Crystal Structure of N,N´-bis-[1-(pyridin-2-yl)ethylidene]-ethane-1,2-diamine
Dinuclear intermolecular H-bonding molybdenum polyimines Schiff base tetracarbonyl
2010/4/8
Multidentate N-ligands (Schiff bases) were prepared by the condensation of 2-acetylpyridine or 2-benzoylpyridine, and 1,2-diaminoethane or 1,6-diaminohexane (2:1 ratio) in ethanol. These ligands were ...
The Mechanism and Crystal Structure of 2-Methoxy-2-methyl-4-phenyl-3,4,4a, 10b-tetrahydro-2H,5H-pyrano[3,2-c]chromen-5-one. Acetal of Warfarin Acid
Warfarin acid synthesis acetal crystal structure
2010/4/19
Acetal of warfarin acid has been synthesized via a hemi acetal intermediate and structurally characterized by X-ray diffraction. The crystal structure shows that the title compound was formed by the h...
Synthesis, Crystal Structure and Antifungal/Antibacterial Activity of Some Novel Highly Functionalized Benzoylaminocarbothioyl Pyrrolidines
Pyrrolidine derivatives aminocarbothioyl derivatives bioactivity antibacterial activity antifungal activity toxicity
2010/4/19
A series of novel highly functionalized benzoylaminocarbothioyl pyrrolidines were prepared from benzoylisothiocyanate and substituted pyrrolidines in excellent yield. The crystal structure of the nove...
Synthesis and Crystal Structure of 1,3-Bis(5-formylpyrrol-2-yl)benzene and Its Conversion to a Macrocyclic Derivative
Schiff Base Bisformylpyrrole Macrocycle Crystal structure
2010/4/19
This report details the synthesis and characterization of a new diformyl pyrrole derivative 2 and its macrocyclic derivative 3. The new compounds were characterized by FT-IR, 13C NMR, and 1H NMR spect...
Crystal Structure of the cis-bis[4-chloro-N-(pyrrolidine-1-carbothioyl)-benzamido] copper(II) Complex
Thioureas X-ray structures Benzoylthiourea complexes Cu(II) complex
2010/4/20
The crystal and molecular structure of the cis-bis[4-chloro-N-(pyrrolidine-1-carbothioyl)-benzamido] copper(II) complex was determined by single-crystal X-ray diffraction. The title compound, C24H24N4...
Crystal Structure of cis-bis(N,N-dimethyl-N'-benzoylthioureato)palladium(II)
Complex X-ray structure single crystal N,N-dimethyl-N'- benzoylthiourea
2010/4/21
In this study cis-bis(N,N-dimethyl-N'-benzoylthioureato) palladium(II) is synthesised and the crystal structure is determined by X-ray diffraction methods. It crystallises in the space group P21/c, wi...
Crystal Structure Effect in Radiation-Induced Solid-State Polymerization of Acrylamide
Crystal Structure Effect Radiation-Induced Solid-State Polymerization Acrylamide
2010/8/15
Crystal structure of arcylamide at -150\circC was studied to understand the role of the crystal structure on the reaction mechanism of radiation-induced polymerization in the solid-state. Acrylamide c...