搜索结果: 16-30 共查到“有机合成化学 Synthesis”相关记录372条 . 查询时间(0.042 秒)
Synthesis and super-swelling behavior of a novel low salt-sensitive protein-based superabsorbent hydrogel: collagen-g-poly(AMPS)
Collagen hydrogel swelling 2-acrylamido-2-methylpropanesulfonic acid
2010/10/19
Superabsorbent polymers are obtained by the graft copolymerization of 2-acrylamido-2-methylpropanesulfonic acid (AMPS) monomer onto collagen, using ammonium persulfate as a free radical initiator in t...
Synthesis and characterization of novel triazol compounds containing a thiophen ring as potential antifungal agents and the structure of 2-(2-hydroxy-2-p-tolyethyl)-5-(thiophen-2-ylmethyl)- 4-(4H-1,2,4-triazol-4-yl)-2H-1,2,4-triazol-3(4H)-one
Synthesis 1,2,4-triazole-3-one NaBH4 LiAlH4 antimicrobial activity
2010/10/18
A series of new 4-(3,5-disubstitue-4H-1,2,4-triazol-4-yl)- 5-(thiophen-2-yl-methyl)-2H-1,2,4-triazol-3(4H)-ones (3a-c) were obtained by reaction N'-1-ethoxy-2-thiophen-2-yl-ethylydene hydrazino carbox...
Heterocyclic synthesis using nitrilimines: part 14. Synthesis of new pyrazole derivatives
Nitrilimines 1,3-dipolar cycloaddition phthalides pyrazoles
2010/10/18
A new series of 1,3,4,5-tetrasubstituted pyrazoles have been synthesized by the 1,3-dipolar cycloaddition of suitable nitrilimines to 3-propylidene and 3-benzylidene-phthalide. Both analytical and spe...
Synthesis and antimicrobial activities of some new biheterocyclic compounds containing 1,2,4-triazol-3-one and 1,3,4-thiadiazole moieties
1,2,4-triazol-3-one 5-thioxo-1,2,4-triazole
2010/10/18
2-(4-Amino-3-(4-chlorophenyl)-5-oxo-4,5--dihydro-1H-1,2,4-triazol- 1-yl)-N'-[(2,6-dihalogenophenyl)-methylene]acetohydrazides (3a,b) was obtained via the formation of 2-(4-amino-3-(4-chlorophenyl)-5-o...
Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
Au nanoparticles ZnO nanorods deposition-precipitation
2010/10/19
Gold nanoparticles supported on zinc oxide nanoparticles were synthesized at several pH levels via the deposition-precipitation (DP) method. The effects of pH on gold loading, particle size, and parti...
Sulfonic acid-functionalized silica: a remarkably efficient heterogeneous reusable catalyst for the one-pot synthesis of 1,4-dihydropyridines
1,4-Dihydropyridine b-dicarbonyl compounds solid acid SiO2-R-SO3H
2010/10/19
An efficient one-pot method for the synthesis of 1,4-dihydropyridines from b-dicarbonyl compounds, aldehyde, and ammonium acetate is reported using sulfonic acid-functionalized silica at 90 °C under s...
Synthesis and characterisation of vanadium(III) complexes of biphenylphenols
Vanadium(III) complexes biphenylphenols magnetic study
2010/10/19
The vanadium(III) complexes of composition [VCl3-n(OAr1,2)n.(THF)2] (OAr1 = 2-phenylphenoxo and OAr2 = 4-phenylphenoxo, THF = tetrahydrofuran; n = 1 /to 3) were prepared by in situ reaction of VCl3.(T...
A new dinuclear lead(II) complex of 2,3-diphenyl-tetrazole-5-thione: synthesis and characterization
Lead complex tetrazole-5-thione crystal structure
2010/10/19
The present work reports on the synthesis, crystal structure, fluorescence, electrochemical behavior, and thermogravimetric analysis of a new dinuclear lead(II) complex of 2,3-diphenyl-tetrazole-5-thi...
Silica supported polyphosphoric acid (PPA-SiO2): an efficient and reusable heterogeneous catalyst for the one-pot synthesis of a -amino phosphonates
a -Amino phosphonates PPA-SiO2 heterogeneous catalyst
2010/10/19
An efficient green protocol is described for the preparation of a -amino phosphonates, employing a one-pot three-component condensation reaction between aldehydes, amines, and trialkyl phosphites in t...
Synthesis and characterization of hybrid congo red from chloro-functionalized silsesquioxanes
Ceramic dye hybrid dye POSS congo red
2010/10/18
Congo red dye has been bonded to the functionalized octameric polyhedral silsesquioxanes (POSS), which were prepared by hydrolytic condensation of chloro-functionalized organosilicon monomers in the p...
Synthesis, characterization, antibacterial and antifungal evaluation of some new platinum(II) complexes of 2-phenylbenzimidazole ligands
Antibacterial activity antifungal activity benzimidazole
2010/10/18
A series of platinum(II) complexes of the type [PtL2Cl2] 1, [PtL2I2] 2, [PtL2(oxalato)] 3, and [PtL2(malonato)] 4 (L= 2-phenylbenzimidazole ligands as ``non-leaving groups'') were synthesized and cha...
An efficient one-pot synthesis of dihydropyrimidinones catalyzed by zirconium hydrogen phosphate under solvent-free conditions
Biginelli reaction solvent-free zirconium hydrogen phosphate
2010/10/18
A simple, efficient, and practical procedure for the Biginelli reaction using zirconium hydrogen phosphate [Zr(H2PO4)2] as a novel solid acid catalyst is described under solvent-free conditions in hig...
Asymmetric synthesis of 8-O-4'-neolignan perseal B
Neolignans perseal B enantioselective synthesis
2010/10/18
Full details of an enantioselective total synthesis of 8-O-4'-neolignan perseal B are presented for the first time. The synthesis was achieved in 8 steps from vanillin and involved the asymmetric dihy...
An efficient synthesis of Schiff bases containing benzimidazole moiety catalyzed by transition metal nitrates
Aldehyde 2-aminobenzimidazole catalyst Schiff bases
2010/10/18
A simple and efficient method has been developed for the synthesis of some novel Schiff bases via the reaction of aromatic aldehydes with 2-aminobenzimidazole by using catalytic amount of M(NO3)2.xH2O...
Convenient synthesis of monomeric steroids from steroidal oxalate dimers using flash vacuum pyrolysis (FVP)
Steroid oxalate dimers steroidal alkene diene triene
2010/10/18
Flash vacuum pyrolysis (FVP) or thermolysis (FVT), an environmentally friendly method for studying organic reaction mechanisms as well as synthesis, was applied to a series of oxalate dimers (1, 3, 5,...