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2,2'-Binaphthylene phosphorochloridite (BINOL-PCl) as a bulky and efficient reagent for the conversion of primary and secondary alcohols into iodides, and tertiary alcohols stereo- and/or regioselectively into olefin(s)
Alkyl iodide 2,2'-dihydroxy-1,1'-dinaphthalene (BINOL) 2,2'-binaphthylene phosphorochloridite (BINOL-PCl) stereoselective anti-E2 elimination reaction heavy atom effect
2010/4/8
Primary and secondary alcohols were transformed in high yield to corresponding iodides by 4-chloro-3,5-dioxaphosphacyclohepta [2,1-a; 3,4-a'] dinaphthalene (BINOL-PCl) at room temperature. The tertiar...
Efficient Method for Tetrahydropyranylation of Phenols and Alcohols Using 2,4,6-Trichloro[1,3,5]triazine
2,4,6- Trichloro[1,3,5]triazine (TT) cyanuric chloride (CC) alcohol phenol tetrahydropyranylation 3,4-dihydro- 2H-pyran (DHP) protection
2010/4/19
Alcohols and phenols were tetrahydropyranylated in the presence of 2,4,6-trichloro[1,3,5]triazine in good to excellent yields in acetonitrile.
A New and Convenient Method of Generating Alkyl Isocyanates from Alcohols, Thiols, and Trimethylsilyl Ethers Using a 2,4,6-Trichloro[1,3,5] Triazine/n-Bu4NOCN
2,4,6-Trichloro[1,3,5] triazine (TT) alcohol thiol trimethylsilyl ether alkyl isocyanate
2010/4/19
Alkyl isocyanates are prepared in good to excellent yields by treatment of alcohols, thiols, and trimethylsilyl ethers with 2,4,6-trichloro[1,3,5] triazine/n-Bu4NOCN in acetonitrile. This method is hi...
An Efficient Acetylation of Primary and Secondary Aliphatic Alcohols with Acetic Anhydride in the Presence of Graphite Bisulphate
Primary and secondary aliphatic alcohols acetic anhydride graphite bisulphate acetylation
2010/6/29
In cyclohexane, thirteen examples of primary and secondary aliphatic alcohols were easily converted to the corresponding acetate derivatives within a short time, ranging from 5 min to 2.5 h, and in go...
Transition Metal Compound Mediated Reduction of a-Amino Acids to 1,2-Amino Alcohols with NaBH4 in Water
Transition Metal Compound Mediated Reduction a-Amino Acids to 1,2-Amino Alcohols NaBH4 Water
2010/6/28
A new efficient and cost-effective method for the preparation of 1,2-amino alcohols is described. The reactions of amino acids with NaBH4 in the presence of NiCl2 or MoO3 in water give 1,2-amino alcoh...