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Synthesis, Spectroscopic Characterization, Mass Spectrometry and Crystal Structure of N-{[(4-bromophenyl) amino]carbonothioyl}benzamide
Thiourea derivative X-ray structure determination mass fragmentation
2010/10/19
N-{[(4-bromophenyl)amino]carbonothioyl}benzamide was synthesized and characterized by IR, 1 H- and 13C-NMR, mass spectrometry, and elemental analysis. The crystal structure was determined from single ...
Synthesis and super-swelling behavior of a novel low salt-sensitive protein-based superabsorbent hydrogel: collagen-g-poly(AMPS)
Collagen hydrogel swelling 2-acrylamido-2-methylpropanesulfonic acid
2010/10/19
Superabsorbent polymers are obtained by the graft copolymerization of 2-acrylamido-2-methylpropanesulfonic acid (AMPS) monomer onto collagen, using ammonium persulfate as a free radical initiator in t...
Conveinient Synthesis and Anion Recognition Property of Acylhydrazone-based Molecular Tweezer Receptors
Anion recognition molecular tweezer acylhydrazone
2010/10/19
Three acylhydrazone-based compounds were designed as novel neutral sensors for anions, and synthesized by simple steps in good yields. Their anion recognition properties were studied by UV-vis and 1H-...
Synthesis and characterization of novel triazol compounds containing a thiophen ring as potential antifungal agents and the structure of 2-(2-hydroxy-2-p-tolyethyl)-5-(thiophen-2-ylmethyl)- 4-(4H-1,2,4-triazol-4-yl)-2H-1,2,4-triazol-3(4H)-one
Synthesis 1,2,4-triazole-3-one NaBH4 LiAlH4 antimicrobial activity
2010/10/18
A series of new 4-(3,5-disubstitue-4H-1,2,4-triazol-4-yl)- 5-(thiophen-2-yl-methyl)-2H-1,2,4-triazol-3(4H)-ones (3a-c) were obtained by reaction N'-1-ethoxy-2-thiophen-2-yl-ethylydene hydrazino carbox...
Heterocyclic synthesis using nitrilimines: part 14. Synthesis of new pyrazole derivatives
Nitrilimines 1,3-dipolar cycloaddition phthalides pyrazoles
2010/10/18
A new series of 1,3,4,5-tetrasubstituted pyrazoles have been synthesized by the 1,3-dipolar cycloaddition of suitable nitrilimines to 3-propylidene and 3-benzylidene-phthalide. Both analytical and spe...
Synthesis and antimicrobial activities of some new biheterocyclic compounds containing 1,2,4-triazol-3-one and 1,3,4-thiadiazole moieties
1,2,4-triazol-3-one 5-thioxo-1,2,4-triazole
2010/10/18
2-(4-Amino-3-(4-chlorophenyl)-5-oxo-4,5--dihydro-1H-1,2,4-triazol- 1-yl)-N'-[(2,6-dihalogenophenyl)-methylene]acetohydrazides (3a,b) was obtained via the formation of 2-(4-amino-3-(4-chlorophenyl)-5-o...
Synthesis and spectroscopic studies of some new organometallic chelates derived from bidentate ligands
4-Amino-5-mercapto-s-triazole Schiff bases silicon complexes
2010/10/18
A series of organosilicon(IV) and organotin(IV) complexes having the formulae R2MCl(L1), R2MCl(L2), R2MCl(L3), R2MCl(L4), R2M(L1)2, R2M(L2)2, R2M(L3)2, and R2M(L4)2, where M = Si and Sn, and R = CH3, ...
Synthesis and characterization of gold nanoparticles supported on zinc oxide via the deposition-precipitation method
Au nanoparticles ZnO nanorods deposition-precipitation
2010/10/19
Gold nanoparticles supported on zinc oxide nanoparticles were synthesized at several pH levels via the deposition-precipitation (DP) method. The effects of pH on gold loading, particle size, and parti...
Sulfonic acid-functionalized silica: a remarkably efficient heterogeneous reusable catalyst for the one-pot synthesis of 1,4-dihydropyridines
1,4-Dihydropyridine b-dicarbonyl compounds solid acid SiO2-R-SO3H
2010/10/19
An efficient one-pot method for the synthesis of 1,4-dihydropyridines from b-dicarbonyl compounds, aldehyde, and ammonium acetate is reported using sulfonic acid-functionalized silica at 90 °C under s...
A simple and efficient procedure for synthesis of optically active 1,3,4-oxadiazole derivatives containing L-amino acid moieties
N-phetaloyl-L-amino acid 1,3,4-oxadiazole diacylhydrazide pyridoyl hydrazide
2010/10/19
Some new unsymmetrical and optically active 2,5-disubstituted 1,3,4-oxadiazoles 5a-j were efficiently synthesized by cyclization reaction of diacylhydrazides 4a-j. The synthesis of the title compounds...
Synthesis and characterisation of vanadium(III) complexes of biphenylphenols
Vanadium(III) complexes biphenylphenols magnetic study
2010/10/19
The vanadium(III) complexes of composition [VCl3-n(OAr1,2)n.(THF)2] (OAr1 = 2-phenylphenoxo and OAr2 = 4-phenylphenoxo, THF = tetrahydrofuran; n = 1 /to 3) were prepared by in situ reaction of VCl3.(T...
A new dinuclear lead(II) complex of 2,3-diphenyl-tetrazole-5-thione: synthesis and characterization
Lead complex tetrazole-5-thione crystal structure
2010/10/19
The present work reports on the synthesis, crystal structure, fluorescence, electrochemical behavior, and thermogravimetric analysis of a new dinuclear lead(II) complex of 2,3-diphenyl-tetrazole-5-thi...
Silica supported polyphosphoric acid (PPA-SiO2): an efficient and reusable heterogeneous catalyst for the one-pot synthesis of a -amino phosphonates
a -Amino phosphonates PPA-SiO2 heterogeneous catalyst
2010/10/19
An efficient green protocol is described for the preparation of a -amino phosphonates, employing a one-pot three-component condensation reaction between aldehydes, amines, and trialkyl phosphites in t...
Synthesis and characterization of hybrid congo red from chloro-functionalized silsesquioxanes
Ceramic dye hybrid dye POSS congo red
2010/10/18
Congo red dye has been bonded to the functionalized octameric polyhedral silsesquioxanes (POSS), which were prepared by hydrolytic condensation of chloro-functionalized organosilicon monomers in the p...
Synthesis, characterization, antibacterial and antifungal evaluation of some new platinum(II) complexes of 2-phenylbenzimidazole ligands
Antibacterial activity antifungal activity benzimidazole
2010/10/18
A series of platinum(II) complexes of the type [PtL2Cl2] 1, [PtL2I2] 2, [PtL2(oxalato)] 3, and [PtL2(malonato)] 4 (L= 2-phenylbenzimidazole ligands as ``non-leaving groups'') were synthesized and cha...